
The
EDL series of Platinum reference thermocouples are offered for use from
0°C to
1450°C and for short-term intermittent measurements up to 1700°C.
Our thermocouples are designed and built to be used as precision standards
and are not meant to be left in the case lying on a shelf. Our construction
method and superior materials result in a highly durable and reliable
reference sensor.
EDL offers three different sheath materials for our line
of Platinum reference sensors; a high purity ceramic, Inconel 600, and
quartz sheaths are available in three standard lengths of 10",
16", and 22" long. Our sensors are also available in three
different diameters as a standard part number. These standard sizes
are .187", .250", and .375" diameters.
A specific combination of diameter and length can be chosen
to fit your calibration furnace or fixed point cells. These probes may
also be used to verify processing readings in virtually any type of
processing equipment from semiconductor wafer fabrication to high temperature
sintering furnaces.
Imperial Units
|
Diameter
|
Tolerence |
Length |
Tolerence |
O.A.L. |
Lead Length |
Replaceable Sheath |
| .187" |
±. 005" |
10" |
± .250" |
15" |
48" |
Yes |
| .250" |
±. 005" |
16" |
± .250" |
22" |
48" |
Yes |
| .375" |
±. 005" |
22" |
± .250" |
27" |
48" |
Yes |
Metric Units
| Diameter |
Tolerence |
Length |
Tolerence |
O.A.L. |
Lead Length |
Replaceable Sheath |
| 4.75 mm |
±.15 mm |
254 |
± 10 mm |
381 |
1200 mm |
Yes |
| 6.34 mm |
±.15 mm |
406 |
± 10 mm |
558 |
1200 mm |
Yes |
| 9.52 mm |
±.15 mm |
558 |
± 10 mm |
685 |
1200 mm |
Yes |
EDL Platinum reference sensors are available with either
a cold end compensation junction or with standard type R/S extension
wire of 48 inches long. Our cold junction connection is made within
a .250" diameter Stainless Steel sheath that may be placed in a
standard Dewar type flask or in an artificial ice point. The lead length
from the sensor to the compensation probe is 24 inches; the compensation
probe has 48 inches of flexible stranded copper ready for attachment
to your instrument. The option code for this feature is a "C"
at the end of the part number.
The lead material for all sensor styles is a Teflon insulated
wire inside of a Stainless Steel armored cable. This construction is
well suited for both the laboratory and shop floor environment. Lead
termination may be added at your facility or we can supply most terminations
for your convenience. To assure an integral seal we use only pure Teflon
glands in the compression-fitting end of the handle to connect the protection
tube to the handle.
General considerations regarding the use of Platinum Rhodium/Platinum
thermocouples:
The thermoelectric power of these thermocouples is relatively
low, but their other physical characteristics generally prove more valuable
to the industrial user. Primarily the behavior of the EMF is quite good
and is considered one of the best for binary alloy thermocouples. The
Platinum is also quite inert and resistant to oxidation that proves
beneficial for many gaseous environments at elevated temperature. The
melting point of Platinum is 1772°C, which makes this thermocouple
useful up to almost 1700°C. Caution must be used above 1450°C
as even short excursions above this temperature will cause premature
grain growth which will promote contamination at the grain boundaries
and will also cause a reduction of tensile strength of the thermo element.
Environmental conditions will also affect long-term stability, requiring
careful consideration of construction materials.
The thermo element will perform well in vacuum, oxidizing,
reducing and inert atmospheres for extended periods provided it is sufficiently
protected by the protection tube. The predominant contributor to drift
will be caused be contamination originating from the sensor itself.
All components of our sensor are well cleaned and carefully assembled
to reduce contamination. We also use only gas tight protection tubes
and 99.8% pure Alumina insulators to reduce cross alloy contamination.
This is an overview of considerations and further discussion may be
required depending on your specific application.
Sheath Material Specifications:
Alumina
Composition . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . . .99.8% (Al2O3)
Impenetrability . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . Gas Tight
Maximum Working Temperature . . . . . . . . . . . . . . . . . . . .
1800°C
Unsupported Sag Temperature . . . . . . . . . . . . . . . . . . . .
.1600°C
Volume Resistivity . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . .>1014
Thermal Conductivity:
@24°C . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . 67.4 WmK
@800°C . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . . . .17.6 WmK
Quartz 214
Composition . . . . . . . . . . . . . . . . . . . . . . . . . .
. . 99.995% (SiO2)
Impenetrability . . . . . . . . . . . . . . . . . . . . . . . . . .
.Gas Tight
Softening Point . . . . . . . . . . . . . . . . . . . . . . . . . .
1683°C
Anneal Point . . . . . . . . . . . . . . . . . . . . . . . . . . . .
.1120°C
Recommended max use temp. . . . . . . . . . . . .1250°C (15 Min.)
Electrical Resistivity . . . . . . . . . . . . . . . . . . . . . .7x109
Ohms/Cm@350°C
Thermal Conductivity:
@24°C . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . ..1.6 WmK
@800°C . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . 1.9 WmK
Inconel 600
Composition . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . Ni76Cr15 (approximate)
Impenetrability . . . . . . . . . . . . . . . . . . . . . . . . . .
. .Gas Tight
Melting Point . . . . . . . . . . . . . . . . . . . . . . . . . . .
. ..1350°C to 1425°C
Recommended max use temp. . . . . . . . . . . . . .1000°C (15 Min.)
Electrical Resistivity . . . . . . . . . . . . . . . . . . . . . . .
103: Ohms/Cm@350°C
Thermal Conductivity @24°C . . . . . . . . . . . . . . ..14.8 WmK
Alumina
The EDL Alumina sheath is 99.8% pure and will withstand temperature
above the melting point of Platinum. This material is impervious to
most chemicals and will not contaminate the working environment due
to evaporation at elevated temperatures. It is more fragile than the
Inconel 600 and will not tolerate shock or side loading. Alumina does
have very high compressive strength. Replacement protection tubes are
available.
G.E. Quartz 214
Our quartz protection tubes offer the most effective solution for
environments requiring virtually no contamination from external sources.
Quartz is an excellent choice for minimizing both hydrocarbon and metallic
ion contamination. The quartz is easily cleaned with alcohol to remove
any contaminants; this is difficult to accomplish with Inconel and Alumina.
In addition due the very high melting point of Platinum there is virtually
no ion contamination potential from the sensor in spite of the transparent
nature of quartz near 1200°C. The quartz is the most fragile protection
tube and will not withstand mechanical shock; it is resistant to thermal
shock. Quartz will also sag as a function of both time and temperature
as it is technically a viscous fluid. This will begin at about 1200°C
after 15 min. and accelerates from this time and temperature. Replacement
protection tubes are available.
Inconel 600
All sheath materials are supplied as gas tight assemblies and can
be used with a vacuum wall feed through. It is recommended that the
Inconel 600 be used for slightly lower temperature applications where
durability is the primary requirement. This material resists oxidation
and is also quite chemically resistant. Consideration should be given
to potential electrical shock should the probe come in contact with
any electrical source, such as a furnace or set of kiln elements. Replacement
protection tubes are quite inexpensive and easily replaced.
Calibration: Platinum 10% Rhodium vs. Platinum
According to the NIST Monograph 175, the temperature to
voltage relationship for Type S thermocouples is described by an eighth
order polynomial and is available in the NIST Monograph 175. The defined
range extends from -50°C to 1768°C. It should be noted that
drift is considerable above 1450°C. In each sub range there is less
than 0.75:V of fit error for the assigned polynomials and their respective
coefficients.
The EDL Platinum sensors are calibrated by comparison
at the ITS90 defined fixed points. The overall achievable uncertainty
for these thermocouples is ±1.0°C. In limited use ranges
±0.5° is an obtainable accuracy. Calibration tables can be
supplied for the sensor ensuring accurate results and eliminating the
need for linear interpolation between calibration points. Please inquire
about this option when placing your order.